Binary Distillation for Process & Chemical Engineering from Udemy

Introduction:

Binary Distillation is one of the most important Mass Transfer Operations used extensively in the Chemical industry.

Understanding the concept behind Gas-Gas, Liquid-Liquid and the Gas-Liquid mass transfer interaction will allow you to understand and model Distillation Columns, Flashes, Batch Distillator, Tray Columns and Packed column, etc...

We will cover:

REVIEW: Of Mass Transfer Basics (Equilibrium VLE Diagrams, Volatility, Raoult's Law, Azeotropes, etc..)
Distillation Theory
Application of Distillation in the Industry
Counter-Current Operation
Several equipment to Carry Gas-Liquid Operations
Bubble, Spray, Packed and Tray Column equipment
Flash Distillation & Flash Drums Design
Design & Operation of Tray Columns
Number of Ideal Stages: McCabe Thiele Method & Ponchon Savarit Method
Recycle
Condenser types: partial, total
Pressure drop due to trays
Design & Operation of Packed Columns
Pressure drop due to trays
Efficiency of Stages & Murphree's Efficency
Batch Distillation, the Raleigh Equation
Software Simulation for Absorption/Stripping Operations (
At the end of the course:
You will be able to understand mass transfer mechanism and processes behind Binary Distillation in Flash, Continuous & Batch Processes. You will be able to continue with a Multi-Component Distillation, Reactive Distillation and Azeotropic Distillation as well as more Mass Transfer Unit Operation Courses and/or Separation Processes Course.
About your instructor:
I majored in Chemical Engineering with a minor in Industrial Engineering back in 2012.
I worked as a Process Design/Operation Engineer in INEOS Koln, mostly on the petrochemical area relating to naphtha treating. There I designed and modeled several processes relating separation of isopentane/pentane mixtures, catalytic reactors and separation processes such as distillation columns, flash separation devices and transportation of tank-trucks of product.

What's inside

Learning objectives

Understand the principles behind binary distillation
Design & operate flashing, and flash drums via flash distillation of binary mixtures
Understand and apply the principles and methods for simple distillation of binary mixtures
Understand continuous distillation equipment
Model distillations of binary systems

Apply mccabe-thiele method for continuous distillation column design (number of stages)
Simulate several process, specially continuous and batch distillation of binary mixtures
Get to know the "recycle ratio", "reboiler duty", "feed stage" etc...
Model stripping and enriching sections of a distillation column

Understand the principles behind binary distillation
Design & operate flashing, and flash drums via flash distillation of binary mixtures
Understand and apply the principles and methods for simple distillation of binary mixtures
Understand continuous distillation equipment
Model distillations of binary systems
Apply mccabe-thiele method for continuous distillation column design (number of stages)
Simulate several process, specially continuous and batch distillation of binary mixtures
Get to know the "recycle ratio", "reboiler duty", "feed stage" etc...
Model stripping and enriching sections of a distillation column

Syllabus

Welcome!

Introduction to Distillation

Requirements

Reference Material

Review of Mass Transfer & Transport Phenomena

Introduction to Section 2

2.1 Ideal Gas

Ideal Solution

Vapor Pressure

Partial Pressure

What is Equilibrium? (Pure Substances)

2.4 Raoult’s Law

What is Flux?

What is Ja? Diffusion Flux

Convection

Types of Unit Equipment

Type of Equipment - Dispersion of Gas-Liquid and Liquid-Gas

Spray Column

Bubble Column

Packed Column

Tray Column

Types of Operation

Single vs. Multiple Stage

Tray Columns

Introduction to Tray Columns

Sieve Trays

Valve Trays

Bubble Cap Trays

Tray Considerations

Trays - Spacing

Trays - Sizing

Trays - Layouts

Trays - Materials

Trays - Manways

Trays - Operations

Tray - Pressure Drop

Trays - Costs

Tray - Maintenance

Trays - Summary

All other Pieces

Bubbling Area

Contact Area

Weir

Downcomer

Stage Efficiency

Murphree's Efficiency

Column Operation - Summary

Tray Diameter Introduction

Tray Spacing

Pressure Drop in Trays

Hd, Dry Liquid sieve loss - Pressure Drop in trays

Hl, (equivalent h eight of clear liquid holdup)

Hd, Surface Tension Pressure loss

Column Operation

Column Operation - Normal

Column Operation - Flooding

Column Operation - Priming

Column Operation - Coning

Column Operation - Weeping

Column Operation - Dumping

Packed Columns

Packed Columns vs. Tray Columns

Introduction to Packings

Packing Material

Stacked Packing

Random Packing

Structural Packing

Other Column Internals

Liquid distributor

Liquid/Vapour Re-Distributor

Demister / Mist Eliminator

Vapour Distributor

Vortex breaker

Packing Supports

Retaining devices (Hold-down Plate & Bed limiter )

Column Structure - Top

Column Structure - Middle

Column Structure - Bottom

Software Simulation

Benzene and toluene Feed Tray, Min. Recycle Ratio, etc

WKS RadFrac - C3 - iC4 Separation - Recycle

WKS RadFrac - Column Internals, Trays vs Packings

WKS Sensitivity Analysis of Feed Stages, Reflux Ratios and Pressure in a RadFrac

Bonus

Top Unit Operation Q&A

BONUS - Continue Your Training!

Good to know

Know what's good

, what to watch for

, and possible dealbreakers

Covers fundamental principles of binary distillation, providing a solid foundation in this essential mass transfer operation

Teaches methods for the design and operation of distillation equipment, such as flash drums and continuous distillation columns

Provides hands-on experience through software simulations, allowing learners to apply their knowledge in practical scenarios

Led by instructors with industry experience in petrochemical applications, ensuring practical relevance

Requires no prerequisites, making it accessible to learners with varying backgrounds

Covers advanced topics such as recycle and condenser types, providing a deeper understanding of distillation processes

Activities

Be better prepared before your course. Deepen your understanding during and after it. Supplement your coursework and achieve mastery of the topics covered in Binary Distillation for Process & Chemical Engineering with these activities:

Review Perry's Chemical Engineers' Handbook

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Reviewing Perry's Chemical Engineers' Handbook will provide you with a comprehensive understanding of the principles and applications of binary distillation.

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Gather the necessary materials
Review the relevant sections
Take notes

Watch Video Lectures on Distillation

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Watching video lectures will help you understand the concepts of binary distillation and how to apply them in practice.

Browse courses on Chemical Engineering

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Find a set of video lectures
Watch the lectures
Take notes

Flash Distillation Tutorial

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Reinforce the principles behind flash distillation through guided tutorials.

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Find a tutorial on flash distillation.
Follow the steps outlined in the tutorial.
Experiment with different feed conditions and operating parameters.

Eight other activities

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Create a Visual Aid

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Creating a visual aid, such as a diagram or flowchart, will help you visualize and understand the process of binary distillation.

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Choose a topic to focus on
Gather information about the topic
Create a visual representation of the information

Join a Study Group

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Joining a study group will allow you to discuss concepts with other students and get help with difficult problems.

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Find a study group
Attend study group meetings
Participate in discussions

Solve Sample Problems

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Solving sample problems will help you practice applying the concepts of binary distillation.

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Find a set of sample problems
Solve the problems on your own
Check your answers

McCabe-Thiele Method Practice

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Practice McCabe-Thiele method to calculate the number of stages required in a continuous distillation column.

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Gather the necessary data, including feed composition, distillate composition, and reflux ratio.
Plot the equilibrium curve and operating line on a McCabe-Thiele diagram.
Step off the stages from the feed point to the distillate point.
Count the number of stages required to achieve the desired separation.

Use Simulation Software

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Using simulation software will allow you to practice designing and operating distillation columns.

Browse courses on Aspen Plus

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Choose a simulation software package
Learn how to use the software
Simulate a distillation process

Tray Column Design

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Demonstrate understanding of tray column design by creating a detailed design document.

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Specify the design criteria, including feed rate, feed composition, and product specifications.
Select the appropriate tray type and determine the number of trays required.
Calculate the tray diameter, spacing, and other design parameters.
Prepare a detailed design document, including drawings and specifications.

Mentor a Junior Student

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Mentoring a junior student will help you solidify your understanding of binary distillation and develop your communication skills.

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Find a junior student to mentor
Meet with your mentee regularly
Help your mentee with their studies

Design a Distillation Column

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Designing a distillation column will allow you to apply the concepts you have learned in this course to a real-world problem.

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Define the problem statement
Gather data
Design the column
Evaluate the design

Career center

Learners who complete Binary Distillation for Process & Chemical Engineering will develop knowledge and skills that may be useful to these careers:

Process Engineer

Process Engineers design, develop, and operate industrial processes. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in many industries.

See salaries and explore the career path for Process Engineer

Chemical Plant Manager

Chemical Plant Managers oversee the operation of chemical plants. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in the chemical industry.

See salaries and explore the career path for Chemical Plant Manager

Process Control Engineer

Process Control Engineers design and implement control systems for industrial processes. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in many industries.

See salaries and explore the career path for Process Control Engineer

Petroleum Plant Manager

Petroleum Plant Managers oversee the operation of petroleum refineries. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate oil and gas from other components.

See salaries and explore the career path for Petroleum Plant Manager

Environmental Plant Manager

Environmental Plant Managers oversee the operation of environmental protection systems. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate pollutants from water and air.

See salaries and explore the career path for Environmental Plant Manager

Chemical Process Operator

Chemical Process Operators operate and monitor chemical plants. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in the chemical industry.

See salaries and explore the career path for Chemical Process Operator

Petroleum Process Operator

Petroleum Process Operators operate and monitor petroleum refineries. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate oil and gas from other components.

See salaries and explore the career path for Petroleum Process Operator

Technical Sales Engineer

Technical Sales Engineers sell and support technical products and services. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in many industries.

See salaries and explore the career path for Technical Sales Engineer

Environmental Process Operator

Environmental Process Operators operate and monitor environmental protection systems. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate pollutants from water and air.

See salaries and explore the career path for Environmental Process Operator

Product Development Engineer

Product Development Engineers design and develop new products. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate and purify products.

See salaries and explore the career path for Product Development Engineer

Research Scientist

Research Scientists conduct research to advance scientific knowledge. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate and purify substances for research purposes.

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Professor

Professors teach and conduct research at universities. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in the chemical industry.

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Chemical Engineer

Chemical Engineers apply physical, chemical, and mathematical principles to design, develop, and operate chemical plants that manufacture products such as pharmaceuticals, plastics, and food. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is a key unit operation in the chemical industry.

See salaries and explore the career path for Chemical Engineer

Petroleum Engineer

Petroleum Engineers design and develop methods for extracting oil and gas from the earth. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate oil and gas from other components.

See salaries and explore the career path for Petroleum Engineer

Environmental Engineer

Environmental Engineers use engineering principles to protect the environment. Binary Distillation for Process & Chemical Engineering may be useful for this role, as it can help build a foundation in the principles of distillation, which is used to separate pollutants from water and air.

See salaries and explore the career path for Environmental Engineer